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17–19 Sept 2018
Fakultät für Maschinenwesen der Technischen Universität München
Europe/Berlin timezone

Combining x-ray emission and x-ray Raman spectroscopy for the study of Earth materials at high pressure and high temperature

17 Sept 2018, 16:30
1h 30m
Fakultät für Maschinenwesen der Technischen Universität München

Fakultät für Maschinenwesen der Technischen Universität München

Boltzmannstraße 15 85748 Garching b. München
Talk MS3 Novel developments in time resolved techniques Poster session 1

Speaker

C. Sternemann (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany)

Description

X-ray emission and x-ray Raman scattering spectroscopy are powerful tools to investigate the local electronic and atomic structure of high and low Z elements in situ and can be applied at high pressure and high temperature conditions which are present in e.g. the Earth's mantle. We developed a setup for simultaneous x-ray emission (Fe Kß$_{1,3}$ and valence to core) and x-ray Raman scattering (low Z elements' absorption edges) studies at beamline P01 of PETRA III synchrotron radiation source using a wavelength dispersive von Hamos spectrometer together with the existing multiple-analyzer Johann-type spectrometer in combination with a laser heating device. It's capabilities are demonstrated by investigating the iron spin crossover in siderite (FeCO$_3$) and bridgmanite ((Mg,Fe)SiO$_3$). This setup provides a unique combination in order to achieve new insights into the spin transition and compression mechanisms of mantle materials which is of importance for the understanding of the macroscopic physical and chemical properties of the inner Earth.

Primary authors

C. Weis (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) G. Spiekermann (Institute of Earth and Environmental Science, Universität Potsdam, Potsdam, Germany) C. Sternemann (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) M. Harder (Deutsches Elektronen-Synchrotron DESY, Hamburg, Germany) R. Sakrowski (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) G. Vankó (Wigner Research Centre for Physics, Hungarian Academy of Sciences, Budapest, Hungary) C. Albers (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) V. Cerantola (European Synchrotron Radiation Facility, Grenoble, France) M. Elbers (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) Y. Forov (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) M. Krstulovic (European Synchrotron Radiation Facility, Grenoble, France) I. Kupenko (Institut für Mineralogie, Universität Münster, Münster, Germany) S. Petitgirard (Bayrisches Geoinstitut, University Bayreuth, Bayreuth, Germany) C.J. Sahle (European Synchrotron Radiation Facility, Grenoble, France) H. Yavaş (Deutsches Elektronen-Synchrotron DESY, Hamburg, Germany) H. Gretarsson (Deutsches Elektronen-Synchrotron DESY, Hamburg, Germany) C. Bressler (European XFEL, Hamburg, Germany) W. Gawelda (European XFEL, Hamburg, Germany) M. Tolan (Fakultät Physik / DELTA, TU Dortmund, Dortmund, Germany) M. Wilke (Institute of Earth and Environmental Science, Universität Potsdam, Potsdam, Germany)

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